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Detail Information
Product Name: | BMK Methyl Glycidate CAS 20320-59-6 Diethyl(nylacetyl)Malonate C15H18O5 | CAS: | 20320-59-6 |
MFï¼ | 206.24 | Type: | Syntheses Material Intermediates |
Appearance: | White Bmk Powder | Sampleï¼ | Availiable |
Chemical Properties
Boiling point : | 120 °C(Press: 0.01 Torr) |
density : | 1.148±0.06 g/cm3(Predicted) |
pka : | 8.76±0.59(Predicted) |
InChI : | InChI=1S/C15H18O5/c1-3-19-14(17)13(15(18)20-4-2)12(16)10-11-8-6-5-7-9-11/h5- 9.13H.3-4.10H2.1-2H3 |
InChIKey : | ZASPDQDIPTZTQQ-UHFFFOYSA-N |
SMILES : | C(OCC)(=O)C(C(CC1=CC=CC=C1)=O)C(OCC)=O |
Basic Information
Synonymsï¼ | Diethyl(nylacetyl)malonate;Propanedioic acid, 2-(2-nylacetyl)-, 1,3-diethyl ester;diethyl 2-(2-nylacetyl)propanedioate;diethyl 2-(2-nylacetyl)propanedioatel;Cas 20320-59-6;Propanedioic acid, (nylacetyl)-, diethyl ester;rmaceutical intermediates Diethyl(nylacetyl)malonate;new p |
CAS: | 20320-59-6 |
MF: | C15H18O5 |
MWï¼ | 278.3 |
EINECSï¼ | 205-854-1 |
Product Categories: | 20320-59-6;BMK |
Mol File: |
Usage and Synthesis
sical properties :
Diethyl(nylacetyl)malonate has a boiling point of 120 °C. Its density is predicted to be 1.148±0.06 g/cm3.
Usesï¼
Organic synthesis intermediates.
Preparationï¼
The anhydrous ethanol co-vaporized with diethyl halate and sodium metal is added dropwise to the mixture of diethyl malonate, carbon tetrachloride and magnesium, heated to start the reaction, and the temperature is controlled to smooth the reaction. Then add anhydrous diethyl ether, heat for 1h, add the diethyl ether solution of nylacetyl chloride (add slowly, not to make the reaction too intense). After the reaction is completed, cool and add water, separate the oil layer, and evaporate the diethyl ether under reduced pressure to obtain diethyl(nylacetyl)malonate.
Company
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